Tiêu chuẩn quốc tế

Số hiệu

Standard Number

ISO 15202-1:2020
Năm ban hành 2020

Publication date

Tình trạng A - Còn hiệu lực

Status

Tên tiếng Anh

Title in English

Workplace air — Determination of metals and metalloids in airborne particulate matter by inductively coupled plasma atomic emission spectrometry — Part 1: Sampling
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Chỉ số phân loại Quốc tế (ICS)

By field

13.040.30 - Không khí vùng làm việc
Số trang

Page

24
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Scope of standard

This document specifies a method for collecting samples of airborne particulate matter for subsequent determination of metals and metalloids using inductively coupled plasma - atomic emission spectrometry (ICP-AES). Samples obtained using the method described herein can also be subsequently analysed for elemental composition by other instrumental methods, such as atomic absorption spectrometry (AAS) or inductively coupled plasma mass spectrometry (ICP-MS).

The method is not applicable to the sampling of mercury, which is present in air in the vapour phase at ambient temperatures; inorganic compounds of metals and metalloids that are permanent gases, e.g. arsine (AsH3); or inorganic compounds of metals and metalloids that are present in the vapour phase at ambient temperatures, e.g. arsenic trioxide (As2O3).

NOTE Although the method does not describe a means of collecting inorganic compounds of metals and metalloids that are present in the vapour phase, in most instances this is relatively easily to achieve by using a back-up filter which has been pre-treated to trap the compound(s) of interest, e.g. a back-up paper pad impregnated with sodium carbonate is suitable for collecting arsenic trioxide (see ISO 11041[2]).

The method is applicable to personal sampling of the inhalable, thoracic or respirable fraction of airborne particles, as defined in ISO 7708, and to static sampling.

This document excludes sampling of surfaces or bulk materials. Guidance on collection of samples for surfaces may be found in ASTM D7659[7].

[2] ISO 11041, Workplace air - Determination of particulate arsenic and arsenic compounds and arsenic trioxide vapour - Method by hydride generation and atomic absorption spectrometry

[7] ASTM D 7659, Standard Guide for Strategies for Surface Sampling of Metals and Metalloids for Worker Protection